Repositório RCAAP

Abstract This study evaluated the effect of microencapsulation and addition of mango peel powder on the survival of Lactobacillus acidophilus and Bifidobacterium lactis, overrun, apparent viscosity, and overall acceptability of symbiotic ice cream during storage at -20 °C for 180 days. Six formulations of vanilla-flavored ice cream were prepared: three with addition of probiotic cultures at a concentration of 108 CFU/g and 0, 2%, and 3% mango peel powder microencapsulated in a sodium alginate matrix, and three with free addition. Analytical evaluations were performed after 1, 30, 60, 90, 120 and 180 days of storage. The results showed that microencapsulation of probiotics and prebiotics statistically influenced (p < 0.05) the characteristics evaluated. The formulation with microencapsulated probiotics and 2% mango peel powder was considered as the best product. This formulation is promising for future commercial application as a functional food because, at the end 180 days of storage, it showed probiotics population >106 CFU/g, 72.97% overrun, 292 mPA apparent viscosity, and good overall acceptance (7.6 points) equivalent to “I like it very much”.

Abstract Serrano artisanal cheese is a traditional raw milk dairy product from southern Brazil. For safe consumption of raw milk products, ripening is a critical period for reducing populations of pathogenic and spoilage microorganism and, then, the knowledge on inactivation kinetics of microorganisms is necessary to guarantee food safety and quality. In the present work, inactivation kinetics of foodborne bacterial pathogens required by Brazilian regulations in serrano artisanal cheeses were statistically evaluated during ripening. The Salmonella spp., Listeria monocytogenes, coagulase-positive strain of Staphylococcus aureus and fecal coliforms were analyzed for up to 60 days. Experimental data were fitted using first-order model, Weibull and log-linear + shoulder models. Results showed no presence of Salmonella spp. and L. monogyatogenes in the cheeses through the studied period. The first-order and Weibull models presented good performance to represent coagulase-positive strain of S. aureus and fecal coliforms during ripening, although Weibull distribution showed better outcomes to experimental data. Log-linear+shoulder equation was discarded to describe the reduction of microorganism counts for physical criteria. Kinetics showed an initial resistance of fecal coliforms to be inactivated, unlike to coagulase-positive strain of S. aureus population. Modeling analysis allowed estimating serrano artisanal cheese ripening period to be longer than 33 days for achieving a safe product according to the Brazilian Regulatory Standards.

Resumo A jabuticaba é nativa da Mata Atlântica do Brasil, sendo uma das frutas mais cultivadas em pomares domésticos, podendo ser consumida in natura ou industrializada. Pela multiplicidade de usos, apresenta apreciável potencial econômico, mas não tem valor comercial alto por ser perecível. Estruturados da polpa concentrada de jabuticaba foram obtidos empregando-se hidrocoloides, como pectina e gelatina, além de edulcorantes, como maltose, sorbitol, glicose e glicerol, considerados supressores da atividade de água. A polpa de jabuticaba e os estruturados obtidos foram caracterizados quanto ao pH, à acidez titulável, à umidade, a sólidos solúveis totais, teor de cinzas, lipídeos, proteínas, açúcares redutores e não redutores e minerais (sódio e potássio). Quanto à análise sensorial foram realizados testes de aceitação e intenção de compra dos estruturados de jabuticaba, obtendo-se boa aceitação dos avaliadores, apresentando índices elevados de intenção de compra. As formulações F1 (contendo glicose, gelatina e pectina) e F4 (contendo sorbitol, gelatina, pectina e maltose) apresentaram diferenças nas proporções de açúcares utilizados, mostrando vantagem em relação às demais formulações, no que diz respeito ao custo para elaboração e ao menor teor de açúcar. Outra vantagem refere-se ao uso de sorbitol, que possui mais poder adoçante comparado à glicose, utilizado na F4, sendo uma alternativa viável para a substituição da glicose, tornando o estruturado mais saudável por conter menor teor de carboidrato. Assim, como as formulações F1 e F4 foram bem aceitas pelos avaliadores, poderiam ser as mais indicadas para a produção pelas indústrias de alimentos.

Abstract Food defense is the effort to protect food from causing harm to the consumer, including security procedures to mitigate intentional acts of adulteration. To assure entry in new markets, food companies need to develop and implement food defense strategies through third-party certification. Although there are some programs designed to assist food business operators in creating effective food defense strategies, this is still not regarded as a priority by food companies. As a first aim of this work, a first-party audit of two meat-producing industries was performed to verify the implementation of food defense requirements. The second purpose of the work was to compare vulnerabilities identified in those two food industries with the ones detected in other previously certified food units in Portugal. For such, a food defense requirements checklist was prepared for the audit and a private certification database was consulted to compare audit results with those from other food business operators certified by at least one international food defense standard. Audit results revealed that both industries were above 50% in overall compliance regarding food defense requirements; still the main vulnerabilities were related to the lack of a food defense plan, the failure to identify critical areas, ineffective warning systems and no training in food defense. Similar vulnerabilities were detected in other certified national food business operators, leading to the conclusion that implementation of food defense requirements seems to be underestimated. As an intervention strategy proposal, food defense training would be of upmost importance to get staff and managers acquainted with the concept.

Abstract The scaling up of the wet process and the design of a coating line to produce edible films, require the consideration of several factors such as, the film formulation, drying kinetics of the films, and the selection of a suitable support material in which to pour the solution. This work aimed to select the most suitable material for the construction of a conveyor belt for the fabrication of edible films through the wet process. The surface properties of the starch film-forming solution were determined. Several commercial materials for conveyor belts were tested. The film-forming solution spreadability and work of adhesion were determined. The mechanical behavior of the dry film was evaluated through mechanical properties and peeling resistance. All materials tested showed good performance under the operational conditions assayed to obtain edible films. Finally, the polyurethane band was chosen due to its appropriate performance and lower cost.

Abstract The benefits of grape consumption are widely recognized and mostly due to phenolic compounds. These beneficial effects will depend on the bioaccessibility of these compounds on grape and its derivatives. This study elaborated two formulations of Isabel grape preparation: PAX (with agave and xylitol) and PS (with sucrose); and two formulations of Isabel grape flour: FAX (from the PAX process residues) and the FS (from the PS process residues). The products were analyzed regarding their nutritional and antioxidant properties; their phenolic compounds’ bioaccessibility was also verified through a simulated digestion model. The preparation and flour exhibited relevant sugars levels (10.83-49.71 g 100 g-1). Those produced with natural sweeteners had a reduction in sugar concentration of 51% and 29% for preparation and flour, respectively, compared to formulations with sucrose, with the high fiber content in the flour is being further highlighted (20.14-21.95 g 100 g-1). The catechin (2.37-28.11 mg 100 g-1) was the most bioaccessible compound (22% to 168%), which together with the caftaric acid (2.31-69.43 mg 100 g-1) and malvidin 3-glucoside (8.65-16.47 mg 100 g-1) represent the compounds observed in greater quantity. The preparations showed higher bioaccessibility regarding grapes and flours for most of the phenolic compounds. Furthermore, the products elaborated presented higher values of anthocyanins and antioxidant activity than the in natura grape, highlighting the beneficial effect of grape processing.

Abstract Indonesian cocoa is cheaper and considered second grade compared with most other cocoa. However, the domestic chocolate industry is not well-developed due to significantly low consumption. To cope with these issues, product innovation through technical process improvement is required to stimulate the domestic chocolate industry. This study aimed to investigate the effect of cocoa bean origin and conching time on the physicochemical (water content, texture, color, crude fat content, and melting enthalpy) and microstructural properties of chocolate. The experiment was conducted under a completely randomized factorial design consisting of two factors: cocoa bean origin (100% fermented cocoa beans from Jember, 100% fermented cocoa beans from Southeast Sulawesi, 50% fermented cocoa beans from Jember + 50% non-fermented cocoa beans from Southeast Sulawesi, and 50% fermented cocoa beans from Southeast Sulawesi + 50% non-fermented cocoa beans from Southeast Sulawesi) and conching time (4, 6 and 8 h). The results showed that cocoa bean origin significantly affected the hardness, gumminess and color of chocolate, including the redness and yellowness level, whereas conching time affected water content, hardness, cohesiveness, elasticity, and crude fat content. Differential scanning calorimetry (DSC) analysis showed that the treatment with 100% fermented cocoa beans from Jember presented higher values of Tonset, ΔHmelt and area compared with those of the treatment with 100% fermented cocoa beans from Southeast Sulawesi, which presented higher values of Tpeak and Tend. Scanning Electron Microscopy (SEM) analysis showed a distribution of solid and dense particles with crystal interaction with chocolate structures.

Resumo Kiwis minimamente processados necessitam de técnicas para manter a qualidade dos frutos durante a conservação e o período de prateleira. Aditivos combinados à radiação ultravioleta podem ser uma alternativa para assegurar a qualidade das frutas por mais tempo de conservação. Neste contexto, foi proposto avaliar a eficiência do uso da radiação UV-C e diferentes aditivos na prevenção do escurecimento e conservação de kiwis ‘Bruno’ minimamente processados. As fatias de kiwi foram submetidas a soluções contendo os seguintes tratamentos: controle, ácido ascórbico a 1%; isoascorbato de sódio a 1%; ácido cítrico a 1%, depois, utilizou-se por dois minutos a radiação UV-C na intensidade de 2,71 kJ m-2. As bandejas foram armazenadas em câmara fria a 4 ± 1 ºC de temperatura, com umidade relativa de 85% a 90%, e armazenadas por períodos de 3, 6 e 9 dias. Avaliaram-se perda de massa, coloração da polpa, sólidos solúveis, acidez titulável, incidência de podridão, compostos fenólicos totais e atividade antioxidante. O uso de aditivos melhora a conservação do kiwi minimamente processado, com destaque para o isoascorbato de sódio e o ácido cítrico. Os frutos de kiwi da cultivar ‘Bruno’ podem ser armazenados por até 6 dias sob refrigeração com o uso de aditivos. Após esse período, a perda de massa é elevada. O uso de UV-C não alterou a qualidade dos kiwis durante o armazenamento, podendo ter seu uso dispensado.

Abstract Finger millet (Eleusine corocana) is a staple cereal grain available in most parts of Africa and India but it is an underutilized and neglected product. It has a low-glycemic index with some nutraceutical advantages. This study aimed to determine the physicochemical characteristics of bread made from wheat and finger millet (FM) composite flours. Wheat flour was blended with FM flour at 10%, 20%, 30% and 40% levels for bread production. Functional properties, pH of composite flours, physical properties and proximate composition of bread were determined. Water and oil holding capacity of flour blends increased from 130.61 to 135.06 and 120.55 to 125.43 g/g, respectively. However, packed and loose bulk density and emulsion stability decreased with inclusion level of FM flour. The pH values of flour blends increased from 5.88 to 6.11. The total color difference of composite bread in terms of crumb and crust increased with the addition of FM flour. Proximate composition of composite bread revealed decrease in moisture and protein contents and increase in ash, fiber, fat contents and carbohydrate at p < 0.05. Incorporation of FM flour decreased the volume and specific volume of bread from 400 to 256.67 mL and 2.69 to 1.81. mL/g, respectively. However, the weight of bread increased from 141.77 to 148.52 g.

Abstract Cowpea grains are nutritious and beneficial to health, contain about 25% of proteins, in addition to carbohydrates, vitamins, minerals, and bioactive compounds. Soaking the beans followed by cooking requires time availability that is incompatible with the current lifestyle. Consumers have opted for read-to-eat, attractive, healthy, nutritious and convenient foods, thus, transforming cowpeas into crispy expanded product is promising. This research aimed to evaluate the effect of the extrusion conditions, moisture, and temperature, on the physical characteristics of the extrudates developed from cowpea cotyledons flour (CCF): from cultivar BRS Guariba (Sorriso, MT, Brazil). The CCF was processed using twin-screw thermoplastic extruder ZSK 30 (Werner & Pfleiderer Co.) varying the moisture (16.2% to 21.8%) and temperature (124 to 166 °C) using Central Composite Rotatable design 22. The expansion index values ranged from 3.01 to 3.98, the regression model was not predictive, with the determination coefficient (r2) equal to 0.67. The independent variables studied presented significant effects, being water solubility index affected by the CCF moisture, compression force (15.63 to 47.72 N) affected by the extruder temperature, the water solubility index (28.34% to 43.67%) by moisture, while the specific volume (2.41 to 4.58 mL g-1) and the water absorption index (5.34 to 6.54 g g-1) were affected for both variables. By simulation, the maximum value of 1 was obtained through the global desirability test in the combination of an extrusion temperature of 124.21 °C and conditioning moisture of CCF of 16.28%. This condition favors obtaining extrudates with greater values for a specific volume and water absorption index, and lower values for compression force and water solubility index.

Resumo Objetivou-se realizar a caracterização físico-química e dos compostos bioativos do extrato aquoso de amendoim sem pele e acrescido de 1% de pele. Os extratos aquosos de amendoim sem e com pele foram caracterizados quanto aos parâmetros: umidade, extrato seco total, cinzas, lipídios, proteínas, teor de sólidos solúveis, acidez titulável, pH, carboidrato e fibras totais, além de compostos fenólicos e flavonoides. Os percentuais de umidade encontrados foram elevados em todas as amostras, resultante de sua base de extrato aquoso produzido na proporção 1:8 (amendoim:água). Observou-se que os extratos aquosos de amendoim sem pele e acrescido de 1% de pele não apresentaram diferença significativa entre si para os parâmetros de pH, como também para sólidos solúveis totais, lipídios e carboidratos. No entanto, a acidez, proteínas, fibras e cinzas apresentaram diferença estatística. Na determinação de compostos fenólicos, notou-se que o extrato aquoso de amendoim com pele apresentou uma quantidade maior quando comparado ao sem pele. Quanto aos flavonoides, a maior quantidade também foi encontrada na amostra com pele, apresentando uma diferença média de 2,52 µg/100 g base úmida. Os extratos aquosos de amendoim com e sem pele mostraram ser uma valiosa alternativa para um melhor aproveitamento do amendoim, proporcionando à população um produto nutricional. A bebida acrescida de 1% de pele enriqueceu o produto quanto ao potencial antioxidante devido às suas maiores concentrações de compostos fenólicos totais e flavonoides.

Abstract Blueberries are widely recognized for their beneficial health effects due to their bioactive compounds content. In addition, balsamic vinegars trade developed quickly because of their wide acceptance in gourmet food. A novel product made with second quality berries, being suitable for human consumption, i.e., blueberry balsamic vinegar, was evaluated. This work aimed to assess changes in Total Anthocyanins (TA), Total Phenolics (TP), and antioxidant activity during production process of blueberry balsamic vinegar, at the following stages: raw material, blueberries juice after enzyme treatment, blueberries alcoholic substrate, blueberries vinegar, concentrated blueberry juice and blueberries balsamic vinegar. Additionally, three alternative evaporation systems, rotary vacuum evaporator, microwave and vacuum microwave, were evaluated in order to determine the concentration method that best retains TA and TP in blueberry juice for its further use in this process. The highest TA and TP retention was achieved by blueberry juice concentration with a rotary vacuum evaporator. On the other hand, both alcoholic fermentation and acetification negatively affected those compounds and antioxidant activity during vinegar production. However, mixing with concentrated juice to obtain blueberry balsamic vinegar allowed balancing nutrient concentration reductions due to processing. The present study showed that production of blueberry balsamic vinegar gives rise to an interesting possibility to reduce losses due to fruit waste while getting added value products with healthy qualities.

Abstract Red beet (or beetroot) is highly nutritious and can be preserved by drying, in order to avoid wastage, to take advantage of crop surpluses, and to add value during the off-season. The objective of this study was to evaluate the effects of osmotic dehydration (OD) and ultrasound (US) pre-treatments on the nutritional quality and sensory characteristics of dried beetroot chips. The kinetics of moisture loss during OD and US were predicted by fitting the experimental data with thin-layer models. The physicochemical parameters (moisture, protein, lipid, carbohydrate, energy, ash, sodium and nitrate) and sensory properties (affective preference-ordering and acceptance test) were determined. Correlations between the treatments and the sensory acceptability evaluated by consumer’s perceptions were performed by applying unsupervised chemometric techniques (Principal Component Analysis (PCA) and Hierarchical Cluster Analysis (HCA)). The two-term exponential model provided the best fit for the experimental drying data. The US treatment promoted a higher drying rate and lower lipid, ash and energy values, while the OD process resulted in higher ash and sodium values. Multivariate analysis revealed that the US and OD treatments improved the sensory properties of the beetroot chips. The US was more efficient pre-treatment for producing beet chips due to its leads a significant reduction on drying time and intermediate level of sensory preference.

Abstract The present study aimed to evaluate the effects of barley malt pomace addition on the characteristics of fresh pork sausages over 10 days of storage. Four fresh sausage formulations were elaborated, one with no addition of barley malt pomace (control formulation), and the other three elaborated with 3%, 6%, and 9% of pomace. The sausages were submitted to physicochemical analyses to determine ash, moisture, protein, lipid, carbohydrate, and raw fiber contents, water activity, pH, peroxide indices, and energetic value. Additionally, texture and color technological analysis and sensory analysis were performed. Sausages with 3% of malt pomace presented a protein content of 17.10% on the 10th day of storage, and raw fiber content of 2.00%; while in the control formulation these contents were 16.59% and 0.77%, respectively, with a significant difference (p ≤ 0.05) between samples, representing an increase in product nutritional value. In the hardness analysis, the control formulation had a value of 13.99 N and the formulation with 3% of pomace of 10.11 N, which shows that sausages with the addition of pomace are not as hard. In the sensory analysis, the control formulation showed about 80% acceptability in all attributes, the sausage with 3% of malt pomace had an acceptability index higher than 80% for the attribute 'global acceptance', the sausage with 6% of pomace had an index of approximately 70% and the formulation with 9% showed acceptability index of approximately 64% for the attribute 'global acceptance'. The addition of 3% of malt pomace to the sausage was the best alternative, since it had good acceptance by consumers, and provided an increased nutritional value. Our results show that the use of malt pomace in meat products is a viable alternative that helps to reduce production costs and aids in solving an environmental issue.

Resumo Na bananicultura, o uso de sacos impregnados por inseticida e a lavagem das pencas são técnicas que visam à qualidade dos frutos. Objetivou-se monitorar, por cromatografia em fase gasosa acoplada à espectrometria de massas, resíduo de bifentrina em bananas lavadas e não lavadas em tanques, assim como na água de lavagem dos frutos. Desde a emissão até a colheita, os cachos foram protegidos com sacos impregnados por bifentrina a 1,0 g kg-1, os quais foram retirados após a colheita, para despencamento e lavagem ou não das pencas em tanques com água, detergente e sulfato de alumínio. Os métodos Quick, Easy, Cheap, Effective, Rugged, Safe Method - QuEChERS e Extração Líquido – Líquido com Partição a Baixa Temperatura - ELL – PBT foram utilizados para extrair resíduo de bifentrina dos frutos no ponto de colheita e maduros, e da água, respectivamente. As porcentagens de recuperação de bifentrina foram 88,16%, 103,4% e 89,32%, na casca, na polpa e em casca + polpa, respectivamente, atendendo à legislação brasileira. No ponto de colheita, na casca e na casca + polpa dos frutos lavados, detectou-se 0,060 mg kg-1 e 0,010 mg kg-1, respectivamente. Quando não lavados, a concentração de bifentrina, na casca, foi de 0,31 mg kg-1 e de 0,16 mg kg-1, na casca + polpa. Não foi detectado resíduo de bifentrina na polpa, independente do estádio de maturação e lavagem, tampouco na água de lavagem. Em frutos maduros não lavados, foram quantificado 0,10 mg kg-1 e 0,040 mg kg1 de bifentrina na casca e em casca + polpa, respectivamente. A lavagem não elimina, mas reduz o resíduo de bifentrina na casca dos frutos no ponto de colheita e, quando maduros, somente os não lavados apresentam resíduo.

Abstract The preparation of bakery products is expanding, mainly due to the possibility of adding other ingredients, in order to enrich them nutritionally. Spinach (Tetragonia tetragonoides) is a vegetable widely used, although its stem that has great potential for use, is still considered a waste and discarded. Based on the aforementioned information, this work aims to elaborate and characterize physical, chemical, sensory and minerals of salty muffins enriched with T. tetragonoides. Four formulations of salty muffins were prepared as following: Standard Formulation (F1); Formulation with addition of spinach leaves (F2); Formulation with addition of spinach stems (F3); Formulation with addition of spinach leaves and stems (F4). The physical and chemical characterization of the leaves and stems of T. tetragonoides was done by quantifying the moisture, residue mineral fixed, proteins, color and minerals. Muffins were characterized by analyzing moisture, fixed mineral residue, protein, total reducing sugars and instrumental analysis of color and texture; sensory and minerals. The muffins showed a predominant green color, due to the addition of spinach. However, stems, leaves and muffins have a high content of minerals, especially calcium and iron. The incorporation of vegetables in the formulations provided an increase in protein content, in addition to expressive sensory acceptance. Feasibility is observed in the production of savory muffins with the addition of leaves and stems, thus using the entire vegetable and avoiding food waste.

Resumo Consumidores têm demonstrado mais atenção à qualidade e à funcionalidade dos alimentos consumidos em razão do aumento da incidência de doenças inflamatórias intestinais, cardiovasculares, hipertensão arterial, diabetes mellitus II, obesidade, cânceres, principalmente aquelas relacionadas à intolerância à lactose e à alergia às proteínas do leite bovino e da soja. Neste estudo, de forma inédita, foram elaboradas e caracterizadas bebidas probióticas à base de extrato de arroz. As bebidas fermentadas com extrato de arroz (BA) foram desenvolvidas com a inoculação de microrganismos Lactobacillus acidophilus, Streptococcus thermophilus e Bifidobacterium animalis ssp. lactis, adoçadas com diferentes tipos de substratos, como sacarose, glicose e mel, e caracterizadas por análises físico-químicas e microbiológicas. Menos tempo de fermentação (nove horas) foi alcançado com a adição do inóculo SAB 440 (Lactobacillus acidophilus, Streptococcus thermophilus e Bifidobacterium animalis ssp. lactis) e da glicose e mel como substratos nas bebidas de extrato de arroz. Todas as bebidas foram caracterizadas como probióticas porque a contagem de células viáveis foi superior a 106 UFC mL-1. Cabe ressaltar que o valor energético pode se enquadrar como baixo, tendo o conteúdo lipídico sido inferior a 0,03%, o que classifica essas bebidas fermentadas como livres de gordura, de acordo com a legislação brasileira vigente. A funcionalidade de bebidas fermentadas elaboradas pode ser atribuída principalmente à sua característica probiótica. As bebidas desenvolvidas são interessantes para o consumo por pessoas intolerantes à lactose e alérgicas a leite de bovino e soja, pois contêm ingredientes não lácteos.

Abstract Broken kernels are among the by-products of processing cashew nuts which have less commercial value. The present work aimed to obtain a cashew kernel protein concentrate from broken kernels, and then characterize it as well as using it in a vegetable burger formulation. The concentrate was obtained by isoelectric precipitation at four different pHs and subsequent drying. Higher yield was 58.6% of proteins (pH 4.0 and 4.5). The concentrate showed Water Absorption Capacity (WAC) of 1.85 mL/g and Oil Absorption Capacity (OAC) of 1.06 mL/g, as well as low solubility in aqueous medium and low foaming capacity. The concentrate was used in vegetable burger production as a substitute for soybean protein. The burgers were submitted to sensory evaluation and obtained an average of 6.6 on a nine-point scale, thus being within the acceptance zone. Regarding the purchase intent, 60% of the judges would probably or would certainly buy the product. Therefore, the cashew kernel protein concentrate can be used as a protein ingredient for food formulation. Producing cashew kernel protein concentrate allows the use of broken kernels generated in the cashew nut industrial process.

Abstract Kuini powders were obtained through spray-drying, freeze-drying, vacuum oven drying and convection oven drying. Colour, water activity (Aw), moisture content, hygroscopicity, wettability, flowability, degree of caking, water solubility index (WSI), total colour change, total phenolic content and total carotenoid content of Kuini powders were determined and compared. Convection oven drying resulted in the highest yield (46.97%), moisture content (4.91%), Aw (0.55) and WSI (74.33%) among all the drying methods. However, convection oven-dried Kuini powder had the lowest hygroscopicity and wettability, which were 18.66% and 12.04 s, respectively. Spray drying resulted in poor hygroscopicity (22.41%), degree of caking (22.16%), wettability (275s), WSI (45.67%) and higher colour change (59.81). Least total colour change (19.05) and higher yellowness (57.31) were observed in freeze-drying. In addition, freeze-dried Kuini powder had the highest total phenolic content (24.76 mg/100 g) and total carotenoid content (1.61 mg/100 g). Drying temperature had a negative and significant correlation with the retention of color pigments and antioxidant content. The physicochemical properties and antioxidant content of freeze-dried Kuini powder were preferred over spray-dried, vacuum oven-dried and convection oven-dried powders. Hence, freeze-drying offers potential application in the food products.

Abstract The production of high quality spirits implies an aging period in wooden barrels, resulting in numerous physicochemical reactions between the wood and the beverage. Oak is the main wood used in the aging process of alcoholic beverages worldwide. However, in Brazil, the use of tropical wood species can be a viable option, allowing for innovation in the characteristics of spirits. This study aimed to determine the aromatic profiling of flavor active compounds in Brazilian sugarcane spirit (cachaça) after a 12-month aging period in new 225-L toasted and non-toasted barrels made from the tropical wood species cerejeira [Amburana cearensis (Fr. Allem.) A.C. Smith], castanheira (Bertholletia excelsa Humboldt & Bonpland), and cabreúva (Myrocarpus frondosus Allemão). The chemical characterization was carried out using the Gas-Chromatography/Mass Spectroscopy (GC/MS) scan mode, and the identification targeted on flavor active compounds (esters, alcohols, organic acids, phenolic compounds, and terpenes). Toasted and non-toasted cerejeira barrels intensified the contents of phenolic compounds in cachaça. The samples aged in cerejeira barrels exhibited the most complex profile, mainly related to organic acids and phenolic compounds. However, cabreúva barrels transferred significant aromatic terpenes to cachaça. This research presented a novel focus on the aromatic profiling of flavor active compounds in cachaça aged in barrels made from tropical wood species.